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It was recently observed that the singular values of the off-diagonal blocks of the matrix sequences generated by the Cyclic Reduction algorithm decay exponentially. This property was used to solve, with a higher efficiency, certain quadratic matrix equations encountered in the analysis of queueing models. In this paper, we provide a sharp theoretical bound to the basis of this exponential decay together with a tool for its estimation based on a rational interpolation problem. Applications to solving block tridiagonal block Toeplitz systems with semiseparable blocks and certain generalized Sylvester equations in arithmetic operations are shown.

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